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Analysing the synthesis and characterization of semi-organic compound tartaric acid ammonium chloride by slow evaporation method


Affiliations
1 Manonmaniam Sundaranar University, Tirunelveli 627 012, India; PG & Research Department of Physics, Annai Velankanni College, Kanyakumari 629 157, India
2 PG & Research Department of Physics, Annai Velankanni College, Kanyakumari 629 157, India
3 Department of Physics, Bethlehem College of Engineering, Kanyakumari 629 157, India

Single crystal synthesis, growth and characterization pose challenges such as impurities, temperature control issues and mechanical stress. The present study aims to address these issues by synthesizing and exploring the physico-chemical properties of a nonlinear semi-organic crystal, tartaric acid and ammonium chloride (TAAC). The crystal growth occurred via the slow evaporation method at ambient temperature using double-deionized water as a solvent. Physico-chemical properties were tested, and characterization included X-ray diffraction, scanning electron microscopy (SEM), and photoluminescence to analyse structure, purity and morphology. Additionally, Fourier-transform infrared spectroscopy, UV-visible spectra and micro hardness methods were employed to analyse the optical properties and determine band-gap energy. Antifungal and antibacterial activities against Candida albicans, Staphylococcus aureus and Pseudomonas aeruginosa were evaluated using the agar-well diffusion method. TAAC demonstrated superior structure and characteristics compared to potassium dihydrogen phosphate crystals across all parameters.

Keywords

Antifungal and antibacterial activity, nonlinear optics, semi-organic compounds, single crystal, slow evaporation method.
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  • Analysing the synthesis and characterization of semi-organic compound tartaric acid ammonium chloride by slow evaporation method

Abstract Views: 17  | 

Authors

T. L. Berlin Beno
Manonmaniam Sundaranar University, Tirunelveli 627 012, India; PG & Research Department of Physics, Annai Velankanni College, Kanyakumari 629 157, India
M. Maria Lenin
PG & Research Department of Physics, Annai Velankanni College, Kanyakumari 629 157, India
R. S. Abina Shiny
Department of Physics, Bethlehem College of Engineering, Kanyakumari 629 157, India

Abstract


Single crystal synthesis, growth and characterization pose challenges such as impurities, temperature control issues and mechanical stress. The present study aims to address these issues by synthesizing and exploring the physico-chemical properties of a nonlinear semi-organic crystal, tartaric acid and ammonium chloride (TAAC). The crystal growth occurred via the slow evaporation method at ambient temperature using double-deionized water as a solvent. Physico-chemical properties were tested, and characterization included X-ray diffraction, scanning electron microscopy (SEM), and photoluminescence to analyse structure, purity and morphology. Additionally, Fourier-transform infrared spectroscopy, UV-visible spectra and micro hardness methods were employed to analyse the optical properties and determine band-gap energy. Antifungal and antibacterial activities against Candida albicans, Staphylococcus aureus and Pseudomonas aeruginosa were evaluated using the agar-well diffusion method. TAAC demonstrated superior structure and characteristics compared to potassium dihydrogen phosphate crystals across all parameters.

Keywords


Antifungal and antibacterial activity, nonlinear optics, semi-organic compounds, single crystal, slow evaporation method.



DOI: https://doi.org/10.18520/cs%2Fv127%2Fi8%2F923-930