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Structural, Thermal and Morphological Studies of the Lanthanum Ferrite Nanopartilces by Amine Combustion Synthesis Method using Hexamine


Affiliations
1 Centre for Nano Science and Technology, I.S.T, Jawaharlal Nehru Technological University-Hyderabad-500 085, India
 

Rare earth metal oxide perovskite structure Lanthanum ferrite nanocrystalline powder was prepared by solution combustion synthesis using Hexamine (HMTA) as a fuel and the fuel to oxidizer ratio is taken as a one (ψ = 1). The lanthanum ferritenanocrystallite was characterized by X-ray Diffraction, thermal gravimetric and differential thermal analyzer and Scanning electron microscopy with Energy dispersive X-ray spectrometer, FTIR and vibrating sample magnetometer.As-prepared nanopowder is observed as orthorhombic structure, thermal stability and morphology studies with elements contain the analysis of the material indicates a fabulous LaFeO3 material is formed. The magnetic properties shows low coercivity and low saturation magnetization for the LaFeO3 nanoparticles.

Keywords

HMTA, Combustion Synthesis, XRD, TG-DTA, SEM with EDAX and VSM.
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  • Structural, Thermal and Morphological Studies of the Lanthanum Ferrite Nanopartilces by Amine Combustion Synthesis Method using Hexamine

Abstract Views: 177  |  PDF Views: 0

Authors

G. Venkaiah
Centre for Nano Science and Technology, I.S.T, Jawaharlal Nehru Technological University-Hyderabad-500 085, India
K. Venkateswara Rao
Centre for Nano Science and Technology, I.S.T, Jawaharlal Nehru Technological University-Hyderabad-500 085, India
V. Sesha Sai Kumar
Centre for Nano Science and Technology, I.S.T, Jawaharlal Nehru Technological University-Hyderabad-500 085, India
Shilpa Chakra
Centre for Nano Science and Technology, I.S.T, Jawaharlal Nehru Technological University-Hyderabad-500 085, India

Abstract


Rare earth metal oxide perovskite structure Lanthanum ferrite nanocrystalline powder was prepared by solution combustion synthesis using Hexamine (HMTA) as a fuel and the fuel to oxidizer ratio is taken as a one (ψ = 1). The lanthanum ferritenanocrystallite was characterized by X-ray Diffraction, thermal gravimetric and differential thermal analyzer and Scanning electron microscopy with Energy dispersive X-ray spectrometer, FTIR and vibrating sample magnetometer.As-prepared nanopowder is observed as orthorhombic structure, thermal stability and morphology studies with elements contain the analysis of the material indicates a fabulous LaFeO3 material is formed. The magnetic properties shows low coercivity and low saturation magnetization for the LaFeO3 nanoparticles.

Keywords


HMTA, Combustion Synthesis, XRD, TG-DTA, SEM with EDAX and VSM.