Open Access Open Access  Restricted Access Subscription Access

ZnO Nanoparticles Synthesis by Sol-Gel Method and Characterization


Affiliations
1 Department of Physics and Nano Technology, SRM University Kattankulathur – 603203, Tamil Nadu, India
 

Background/Objective: ZnO nanoparticle synthesis by sol gel method and its characterization to find out the morphology of the particles.

Methods/Statistical analysis: Sol-gel technique was used to prepare zinc oxide nanoparticles. The characterization was done by X-Ray diffractive (XRD), UV- Visible spectroscopy and field emission scanning electron microscopy (FE-SEM). X-Ray diffraction (XRD) was used to find out the particle size and FE-SEM image was used to determine its morphology.

Findings: pH 9 offers better morphology and good crystalline nature. The morphology can be changed by varying the solvent ratio.

Improvements/Application: Gas sensor application.


Keywords

ZnO Nanoparticle, XRD, FE-SEM, UV Visible, Sol Gel Method.
User
Notifications

  • Ghaida S. Muhammed. Efficiency Enhancement of Crystalline Silicon Solar Cell by the Deposition of Undoped ZnO Thin Film. Indian Journal of Science and Technology. 2011; 4(6), 677-680.
  • Hamid Reza Ghorbani, Ferdos parsa mehr, Hossein pazoki, Brhrad mosavar Rahmani. Synthesis of ZnO Nanoparticles by Precipitation method. Oriental Journal of Chemistry. 2015; 31(2), 1219-1221.
  • M. Mousavi, A. Kompany, M. Rezaee Roknabad, H. Arabshahi. Theoretical Investigation of Electrical and Mechanical Properties of ZnO Crystal. Indian Journal of Science and Technology. 2010; 3(6), 630-633.
  • Hiral Soni, J.I.Nirmal Kumar, Khushal Patel, Rita N. Kumar.Photo-catalytic decolouration of Rhodamine B dye using ZVI nanopowder synthesized by chemical reduction method. Indian Journal of Nanoscience. 2015; 3(2), 1-6.
  • Z. Harith, N. Irawati, M. Batumalay, H. A. Rafaie, G. Yun II, S. W. Harun, R. M. Nor, H. Ahmad. Relative Humidity Sensor Employing Optical Fibers Coated with ZnO Nanostructures. Indian Journal of Science and Technology. 2015; 8(35), 1-5.
  • R. Y Houng, J.H Li. Synthesis and surface modification and photocatalytic properties of ZnO nanoparticles. Powder Technology. 2009; 189, 426-433.
  • R. Yousefi, B. Kamaluddin. The effect of annealing temperature on structural and optical of s-doped ZnO nanobelts. Solid state science. 2010; 12, 250-259.
  • Riyadh M. Alwan, Quraish A. Kadhim. Synthesis of Zinc Oxide Nanoparticles via Sol-Gel Route and Their Characterization, national centre for packing, Iraqi. Nanoscience and Nanotechnology. 2015; 5(1), 1-6.
  • J. Wang, N. Shi, Y. Qi, M. Liu, Reverse micelles template assisted fabrication of ZnO hollow nanospheres and hexagonal microtubes by a novel fast microemulsion-based hydrothermal method, Journal of Sol- Gel Science and Technology. 2009; 53, 101-106.
  • P.G. Surye. Synthesis and characterization of ZnO nanoparticles by sol-gel process, Master of science in physics, National Institute of technology Rourkela, Orissa, India. 2012; 1-36
  • A.Z. Khorsand, R. Razali, W.H. Majid. Synthesis and characterization of narrow size distribution of ZnO nanoparticles. International journal of nanomedicine. 2011; 6, 1396-1403.
  • R. Garcia Gutierrez, M. Barboza Flores. Luminescence and structural of ZnO grown by Physical vapor deposition. Advanced in Materials science in Engineering Journal. 2012; 5.
  • Arun. S. Menon, Nandakumar, Sabu Thomas. Studies on structural and optical properties of ZnO and Mn – doped ZnO nanopowder, Centre for nanoscience and nanotechnology – M.G University, Kottayam. Indian Journal of Nanoscience. 2013; 1(1), 16-24.
  • M. Mashaly, R. A. Abdelghaffar, Magda M. Kamel, B. M. Youssef. Dyeing of Polyester Fabric Using Nano Disperse Dyes and Improving their Light Fastness Using ZnO Nano Powder. Indian Journal of Science and Technology. 2014; 7(7), 960-967.
  • M. Mohammadi, M. Rezaee Rokn-Abadi, H. Arabshahi. Investigations on Impact of Post-heat Temperature on Structural, Optical and Electrical Properties of Al-doped ZnO Thin Films Prepared by Sol-gel Method. Indian Journal of Science and Technology. 2010; 3(2), 110-112.

Abstract Views: 428

PDF Views: 260




  • ZnO Nanoparticles Synthesis by Sol-Gel Method and Characterization

Abstract Views: 428  |  PDF Views: 260

Authors

Deepak Davis
Department of Physics and Nano Technology, SRM University Kattankulathur – 603203, Tamil Nadu, India
Sheela Singh
Department of Physics and Nano Technology, SRM University Kattankulathur – 603203, Tamil Nadu, India

Abstract


Background/Objective: ZnO nanoparticle synthesis by sol gel method and its characterization to find out the morphology of the particles.

Methods/Statistical analysis: Sol-gel technique was used to prepare zinc oxide nanoparticles. The characterization was done by X-Ray diffractive (XRD), UV- Visible spectroscopy and field emission scanning electron microscopy (FE-SEM). X-Ray diffraction (XRD) was used to find out the particle size and FE-SEM image was used to determine its morphology.

Findings: pH 9 offers better morphology and good crystalline nature. The morphology can be changed by varying the solvent ratio.

Improvements/Application: Gas sensor application.


Keywords


ZnO Nanoparticle, XRD, FE-SEM, UV Visible, Sol Gel Method.

References