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Chandrasekaran, A.
- Survey of Stem Wilt Disease of Casuarina Equisetifolia Forst. Incited by Trichosporium vesiculosum Butler. in Tamil Nadu
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Indian Forester, Vol 132, No 9 (2006), Pagination: 1207-1210Abstract
No abstract- Mineral Analysis of Coastal Sediment Samples of Tuna, Gujarat, India
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Authors
Affiliations
1 PG & Research Dept. of Physics, Govt. Arts College, Tiruvanamalai-606601, TN, IN
2 Dept. of Physics, University College of Engg., Arani-632317, TN, IN
3 Dept. of Physics, St.Joseph’s College of Engg., Chennai-119, TN, IN
4 Department of Physics, Sacred Heart College, Thirupattur-635601, TN, IN
5 National Institute of Ocean Technology, Pallikaranai, Chennai -601302,TN, IN
1 PG & Research Dept. of Physics, Govt. Arts College, Tiruvanamalai-606601, TN, IN
2 Dept. of Physics, University College of Engg., Arani-632317, TN, IN
3 Dept. of Physics, St.Joseph’s College of Engg., Chennai-119, TN, IN
4 Department of Physics, Sacred Heart College, Thirupattur-635601, TN, IN
5 National Institute of Ocean Technology, Pallikaranai, Chennai -601302,TN, IN
Source
Indian Journal of Science and Technology, Vol 3, No 7 (2010), Pagination: 775-781Abstract
Qualitative analysis was carried out to determine the major and minor constituent minerals present in sediment samples collected at the coastal area of Tuna, Gujarat by FT-IR and XRD technique. From the IR absorption band or the locations of the different peaks, the minerals were identified with the available literature. In addition to the band positions, the sharpness or diffuseness of bands was helpful in the identification of mineral components. The IR study on sediment samples was highly useful in identifying the various minerals in sediments. Further, the representative sediment samples were analyzed by XRD technique to yield more information about the minerals. Both of these methods were non-destructive and can be used in the identification of mineralogical composition. These results confirmed that the applied techniques are relatively quicker and more reliable in mineral analysis.Keywords
Sediment Samples, Mineral Analysis, FT-IR, XRD TechniqueReferences
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- Benedetto GED, Laviano R, Sabbatini L and Zambonin PG (2002) Infrared spectroscopy in the mineralogical characterization of ancient pottery. J. Cul. Her. 3, 177–186.
- Chester R and Elderfield H (1967) The application of infrared absorption spectroscopy to carbonate mineralogy. Sedimentology. 9, 5-21.
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- Reig FB, Adelankndo JVG and Moreno MCM (2002) FT-IR Quantitative analysis of calcium carbonate (Calcite) and Silica (Quartz) mixtures using the constant ratio method; application to geological samples. Talanta. 58, 811-815.
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- Determination of Firing Temperature of Some Ancient Potteries of Tamil Nadu, India by FT-IR Spectroscopic Technique
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Authors
Affiliations
1 PG & Research Dept. of Physics, Govt. Arts College, Tiruvanamalai-606601, TN, IN
2 Dept. of Physics, St.Joseph’s College of Engineering, Chennai-119, TN, IN
3 Dept. of Physics, Sacred Heart College, Thirupattur-635601, TN, IN
4 Dept. of Physics, C.Abdul Hakeem College, Melvisharam- 632509, TN, IN
5 Dept. of Ancient History and Archeology, University of Madras, Chennai-600005, TN, IN
1 PG & Research Dept. of Physics, Govt. Arts College, Tiruvanamalai-606601, TN, IN
2 Dept. of Physics, St.Joseph’s College of Engineering, Chennai-119, TN, IN
3 Dept. of Physics, Sacred Heart College, Thirupattur-635601, TN, IN
4 Dept. of Physics, C.Abdul Hakeem College, Melvisharam- 632509, TN, IN
5 Dept. of Ancient History and Archeology, University of Madras, Chennai-600005, TN, IN
Source
Indian Journal of Science and Technology, Vol 3, No 9 (2010), Pagination: 1016-1019Abstract
Archaeological artifacts such as potteries, bricks and tiles are the source of information about the ancient civilization, their technological skills and cultural trade etc. Pottery is one of the oldest human technology and art-form that remains as a major industry even today. The potteries are made of clay minerals and kaolinte is the common mineral in pottery making. The firing temperature of ancient potteries is based primarily on changes of physical characteristics occurring when clay minerals are heated. The study of thermal transformations of the clay minerals can thus help in determining the firing temperatures of the potteries. In the present work, the estimation of firing temperature of the recently collected potteries from Melchittamur of Tamil Nadu is determined by FT-IR spectroscopic technique. The mineral composition and firing condition are inferred from the FT-IR spectrum. To estimate the upper limit of firing temperature of pottery fragments, the specimens were refried at different temperatures and the FT-IR spectrum was recorded from the samples. The interpretation of results is made from the IR characteristics absorption bands. Results are discussed and the conclusion is drawn.Keywords
Ancient Pottery, Clay, FT-IR, Firing TemperatureReferences
- Clarence Karr. Jr (1974) Infrared and Raman spectroscopy of Lunar and terrestrial minerals. Academic Press, NY, pp: 325-358.
- De Benedetto, Fabbri B, Sabbatini L and Zambonin PG (2002) Infrared spectroscopy in the mineralogical characterization of ancient pottery. J. Cult. Heritage. 3, 177–186.
- Eissa NA, Sallam HA, Sanad AM and Mira AF (1979) Application of Mossbauer spectroscopy in investigating Egyptian archaeology. Ind. J. Pure. Appl. Phys. 17, 731- 737.
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- Kanchan DK, Mendiratta RG and Puri RK (1986) an Infrared study of the 20Na -V2O5-Fe2O3 Glass system. J. Mat. Sci. 21, 2418-2422.
- Longworth G and Tite MS (1977) Mossbauer and magnetic susceptibility studies of Iron oxides in soils from archaeological sites. Archaeometry. 19, 3-14.
- Lyon RJP (1967) Infrared absorption spectroscopy, physical methods in determinative mineralogy. Zussman J (Ed.), Academic Press, NY, pp: 371-403.
- Makundi IN, Waern Sperber A and Ericson T (1989) Studies of archaeological problems by Mossbauer spectroscopy. Archaeology. 31, 54-65.
- Maniatis Y, Katsanos ME and Caskey K (1982) Analysis of Copper alloys by proton beams. Archaeometry. 24, 191-198.
- Maniatis Y, Simopoulous A and Kosgikas (1981) Mossbauer study of the effect of calcium content on Iron oxide transformations in fired clays. J. Am. Ceram. Soc. 64, 263.
- Maniatis Y, Simopoulous A, Kosgikas R and Perdikastsis V (1983) Effect of a reducing atmosphere on minerals and iron oxides developed in fired clays: the role of Calcium. J. Am. Ceram. Soc. 66, 773.
- Mendeluvici E, Yariv SH and Villaba R (1979) Febearing kaolinite in Venezuelan Laterites: Infrared spectroscopy and chemical dissolution evidence. Clay minerals. 14, 323-331.
- Miller JG (1961) An Infrared spectroscopic study of the isothermal dehydroxylation of kaolinite at 470 0C. J. Phys. Chem. 63, 800-804.
- Palnivel R and Velraj G (2003) Porosity measurements to estimate the firing temperature of ancient potteries. J. Curr. Sci. 3(1), 63-66.
- Prost R, Dameme E, Driard J and Leydecadsker JP (1989) Clays and clay minerals. 37, 464– 468.
- Ramasamy K and Kamalakannan M (1987) Infrared study of some south Indian clays. Ind. J. Pure Appl. Phys. 25, 284-286.
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- Ravisankar R (2009) Application of spectroscopic technique for the identification of minerals from Beach rocks of Tamil Nadu, India. EARFAM. 19, 272-276.
- Ravisankar R, Senthilkumar G, Kiruba S, Chandrasekaran A and Jebakumar PP (2010) Mineral analysis of coastal sediment samples of Tuna, Gujarat, India. Ind. J. Sci. Tech. 3(7), 775-781.
- Ross CS and Kerr PE (1931) The Kaolin minerals. US Geol. Survey Profess. Paper 165 E ,151- 176.
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- Velraj G, Janaki K, Mohamed Musthafa A and Palanivel R (2009) Estimation of firing temperatue of some archaeological pottery shreds from India. Spectrochimica. Acta Part A: Mol. Biomol. Spec. 72, 703-707.
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- Analysis of Ancient Potteries of Tamilnadu, India by Spectroscopic Techniques
Abstract Views :333 |
PDF Views:127
Authors
Affiliations
1 Post Graduate & Research Dept. of Physics, Government Arts College, Tiruvanamalai-606601, TN, IN
2 Department of Physics, St.Joseph’s College of Engineering, Chennai-119, Tamilnadu, IN
3 Department of Physics, Sacred Heart College, Thirupattur-635601, Tamilnadu, IN
4 Department of Physics, University College of Engineering, Arani-632317, Tamilnadu, IN
5 Anthropology Section, Government Museum, Egmore, Chennai-600008,Tamilnadu, IN
1 Post Graduate & Research Dept. of Physics, Government Arts College, Tiruvanamalai-606601, TN, IN
2 Department of Physics, St.Joseph’s College of Engineering, Chennai-119, Tamilnadu, IN
3 Department of Physics, Sacred Heart College, Thirupattur-635601, Tamilnadu, IN
4 Department of Physics, University College of Engineering, Arani-632317, Tamilnadu, IN
5 Anthropology Section, Government Museum, Egmore, Chennai-600008,Tamilnadu, IN
Source
Indian Journal of Science and Technology, Vol 3, No 8 (2010), Pagination: 858-862Abstract
We report the spectroscopic investigation of ancient potteries excavated in Tamilnadu. Qualitative analyses were carried out to determine the major and minor constituent minerals present in the samples based on the band position or location of IR absorption peaks. From the prominent i.r. absorption peaks, the minerals were identified from the available literature. The constituents of minerals present in the potteries are further confirmed by XRD technique. Both FT-IR and XRD techniques reveals the mineral composition of ancient potteries. Energy dispersive X-ray fluorescence (XRF) was used to determine the major, minor and trace element composition of potsherds of ancient potteries. The concentration of trace elements is helpful for the characterization of pottery produced in a given region. The combined techniques are very much useful for the characterization of potteries.Keywords
Ancient Pottery, Mineral Analysis, FT-IR, XRD, EDXRF, Elemental AnalysisReferences
- Benedetto GED, Laviano R, Sabbatini L and Zambonin PG (2002) Infrared spectroscopy in the mineralogical characterization of ancient pottery. J.Cul.Her. 3, 177–186.
- Chester R and Elderfield H (1967) The application of infrared absorption spectroscopy to carbonate mineralogy. Sedimentology.9, 5- 21.
- Chester R and Green RN (1968) The infrared determination of quartz in sediments and sedimentary rocks. Chem.Geo, 3, 199 -212.
- Clarence Karr. Jr (1974) Infrared and Raman Spectroscopy of lunar and terrestrial minerals. Academic Press, NY. pp: 325 -358.
- Clark RN, King TVV, Kiejwa M, Swayze, G.A. and Verge, N (1990) High spectral resolution reflectance spectra of minerals, J.Geophys Res. 95, 12653-12657.
- Coates JP (1977) The IR analysis of quartz and asbestos. Nelioth Offset Ltd., Chesham, England.
- Crowley JK and Vergo N (1988) Near- infrared reflectance of mixtures of kaolin group minerals; use in clay. Clay & Clay Minerals. 36, 310-316.
- Farmer VC (1974) The IR spectra of minerals. Mineralogical Soc., London, 42, 308-320.
- Farmer VC (1979) Infrared spectroscopy. Data hand book for clay materials and other non-metallic minerals. Ed.Van Olphen & Fripait, I Ed., Pergaman Press, Oxford, London. pp: 285 -337.
- Ghosh SN (1978) Infrared spectra of some selected minerals, rocks and products. J.Mat.Sci. 13, 1877-1886.
- Hlavay J, Jonas K, Elek S and Inczedy J (1978) Characterization of the particle size and the crystallinity of certain minerals by infrared spectrophotometry and other instrumental methods-II. Investigation on quartz and feldspar. Clay and Clay Minerals. 26, 139- 143.
- Ko TH and Chu H (2005) Spectroscopic study on sorption of hydrogen sulfide by mean of red soil. Spectro Chimica Acta. Part- A, 61, 2253–2259.
- Lyon RJP (1967) Infrared absorption spectroscopy. In: Physical methods in determinative mineralogy. Zussman J (Ed.), Academic Press, NY. pp:371-403.
- Madejova and Komadel (2001) Baseline studies of the clay minerals society source clays: Infrared methods. Clay & Clay Minerals. 49, 410-432.
- Neog AK, Boruah RK, Sahu OP, Borah PC, Ahmed W and Boruah GD (1999) XRD and IR of Deopani clay. Asian.Chem.Letts. 3,172-175.
- Ravisankar R (2009) Application of spectroscopic technoqies for the identification of minerals from beach rocks of Tamilnadu, India. Exploration & Res. for Atomic Minerals. 19, 272-276.
- Ravisankar R, Rajalakshmi A and Manikandan (2006) Mineral characterization of soil samples in and around saltfield area, Kelambakkam, Tamilnadu, India. Acta Ciencia Indica. Vol.XXXII, (3), 341 – 346.
- Reig FB, Adelankndo JVG and Moreno MCM (2002) FTIR Quantitative analysis of Calcium Carbonate (Calcite) and Silica (Quartz) mixtures using the constant ratio method; Application to geological samples. Talanta. 58, 811-815.
- Russell JD (1987) Infrared methods. In: A hand book of determinative methods in clay mineralogy, Wilson MJ (Ed.) Blackie & Son Ltd, NY, pp: 11-67
- SenthilKumar P, Parthasarathy G, Sharma DS, Srinivasan R and Krishnamurthy P (2001) Mineralogical and geochemical study on carbonate veins of Salem- Attur fault zone, Southern India: Evidence for Carbonate affinity. J.Geo.Soc.Ind. 58, 15-20.
- Sevim Akyuz, Tami Akyuz, Sait Basaran and Ahmet Gulec (2008) Analysis of ancient potteries using FT-IR, micro-Raman and EDXRF spectrometry. Viberational Spectrocopy. 48, 276-280.
- Summer ME (1995) Hand book of soil science. Univ. of Georgia, Boca Raton Hondor Press, NY.
- White JL (1971) Interpretation of infrared spectra of soil minerals. Soil science, 112, 22-67.
- Xu Z, Cornilsen BC, Popko DC, Penning WD, Wood JR and Hwang JY (2001) Quantitative mineral analysis by FT-IR spectroscopy. Int.J.Vib.Spec. 5, 4-6.