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Differentiation Roselle (Hibiscus Sabdariffa L.) Extract from Various Plants with FTIR-chemometric Method


Affiliations
1 Department of Pharmaceutical Biology, Faculty of Pharmacy, Padjadjaran University, Jalan Raya Bandung- Sumedang KM 21, Jatinangor, West Java,, Indonesia
2 Department of Pharmaceutical Analysis and Medicinal Chemistry, Faculty of Pharmacy, Padjadjaran University, Jalan Raya Bandung- Sumedang KM 21, Jatinangor, West Java,, Indonesia
     

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Background: Roselle prospectively can be developed as herbal medicine raw materials. The high amount availability of roselle raw material sources leads to diverse roselle extract quality therefore a particular method is required to differentiate roselle extracts. FTIR-chemometric is a method that is used to evaluate plant quality by processing chemical data information through mathematically and statistically calculations. Aim: The purpose of this study is to obtain data differentiation from all of the roselle extract obtained from various regions, identify from which region roselle extract has similar group with roselle standard extract, and identify the relation between roselle extracts quality with soil examination parameter. Materials and Method: Roselle simplisia collections were obtained from 12 regions which were Parangtritis, Nganjuk, Kediri, Ponorogo, Blitar, Bogor, Tulungagung, Boyolali, Yogyakarta, Sukabumi, Cileunyi, dan Malang. The extraction method used was using maceration with 70% ethanol. FTIR-chemometric was utilized to analyze. Results: Based on the results showed that FTIR-chemometric method can be used to differentiate roselle extract from several locations, roselle extract obtained from Tulungagung, Boyolali, and Sukabumi were in similar group with roselle extract standard, and roselle extract obtained from Tulungagung, Boyolali, and Sukabumi had similar soil examination parameter which were Phosphorus and Magnesium.

Keywords

Roselle, FTIR-chemometric, Soil parameter.
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  • Badreldin, H. A., Naser Al, W. and Gerald, B. Phytochemical, pharmacological and toxicological aspects of Hibiscus sabdariffa L.: a review. Phyther. Res. 2005. 19, 369–375

  • Li, S. et al. Chemical markers for the quality control of herbal medicines: An overview. Chinese Medicine. 2008; doi:10.1186/1749-8546-3-7.

  • Mok, D. K. W. and Chau, F. T. Chemical information of Chinese medicines: A challenge to chemist. Chemom. Intell. Lab. Syst. 2006; doi:10.1016/j.chemolab.2005.05.006.

  • Rohman, A., Nugroho, A., Lukitaningsih, E. and Sudjadi. Application of vibrational spectroscopy in combination with chemometrics techniques for authentication of herbal medicine. Applied Spectroscopy Reviews. 2014. doi:10.1080/05704928.2014.882347.

  • Sun, S., Chen, J., Zhou, Q., Lu, G. and Chan, K. Application of mid-infrared spectroscopy in the quality control of traditional Chinese medicines. Planta Medica. 2010. doi:10.1055/s-0030-1250520.

  • Shirsat, N. D., Momin, P. S. A., Bandekar, A. A. and Sayed, U. Synthesis of Water Soluble Chitosan from Marine Waste and Its Application in Wet Wipes Formulations. 2012. 5, 1419–1423

  • Khan, B. Synthesis and Characterization of Ter-Butyl Chloride and Its Derivatives (Ter-Butyl Zinc Chloride and Ter-Butyl Lead Chloride) By Using TLC, FTIR, UV/VIS and GC/MS Techniques. 2010. 3, 1011–1014.

  • Gandhi, S. V. and Sonawane, P. S. Chemometric-Assisted UV Spectrophotometric Method for Determination of Cefixime Trihydrate and Cloxacillin Sodium in Pharmaceutical Dosage Form. 2018. Asian J. Res. Chem. 11, 705.

  • Gad, H. A., El-Ahmady, S. H., Abou-Shoer, M. I. and Al-Azizi, M. M. Application of chemometrics in authentication of herbal medicines: A review. Phytochemical Analysis. 2013. doi:10.1002/pca.2378.

  • Zou, H. Bin et al. Progress in quality control of herbal medicine with IR fingerprint spectra. Analytical Letters . 2005. doi:10.1081/AL-200062153.

  • Perawati, S., Yasmiwar, S., dan Sumiwi, S. Isolasi senyawa antihipertensi dari fraksi etil asetat kelopak bunga rosela (Hibiscus sabdariffa L.) terhadap tikus putih jantan galur wistar. (Unpad, Bandung, 2016).

  • Depkes RI. Farmakope Herbal Indonesia Edisi I. Farmakope Herbal Indonesia (2008).

  • Tyagi, S., Alam, T., Khan, M. A., Tarannum, H. and Chauhan, N. Biosynthesis of silver nanoparticles using medicinal plant Anacyclus Pyrethrum and its antibacterial efficacy. Asian J. Res. 2018. Chem. 11, 515 .

  • Pawar, P. H. and Chaudhari, S. R. Size controlled Bio-directed synthesis of Ag Metal Nanoparticles using Tulsi ( Ocimum tenuiflorum ) leaves extract . Asian J. Res. 2017. Chem. 10, 646.

  • Akhtar, K., Ranjan, R. and Alam, M. Oxidative Degradtion and Associated Complexation of Ethylacetoacetate by Cr (VI) Based Oxidant. Asian J. Res. 2012. Chem. 5, 191–192.

  • Hoang, V. D. Chemometrics-assisted Spectrophotometric Determination of Ciprofloxacin and Naphazoline in Eye Drops. 2014. 7, 461–465.

  • Mohan, G. V. K., Rao, K. K. and Rao, P. V. V. P. Environmental impact assessment of sediment quality analysis of Bhavanapadu mangrove ecosystem, East Coast of India. Asian J. Res. 2011. Chem. 4, 1067–1072.

  • Jyoti A. K and Sureshbhai. P. Effects of Nutrients in Soil Analysis of Shirpur Tahasil Region. 2010. 3, 596–599.

  • Telkapalliwar, N. G., Borikar, D. M. and Shivankar, V. M. Physico-chemical characterization of farmland soil samples of nearby villages of Hingna Taluka, district Nagpur, Maharashtra, India. 2017. Asian J. Res. Chem. 10, 301.

  • Hakim. N, M.Y. Nyakpa, A.M. Lubis, S.G Nugroho, M.R. Saul, M.H. Diha G.B. Hong, H. H. B. Dasar-Dasar Ilmu Tanah. (1986).

  • Ginting, E. N., Sutandi, A., Nugroho, B. and Indriyati, L. T. Rasio dan kejenuhan hara k, ca, mg di dalam tanah untuk tanaman kelapa sawit (elaeis guineensis jacq). J. Ilmu Tanah dan Lingkung. 2013. doi:10.29244/jitl.15.2.60-65.

  • Portal Sukabumi. 2018. (Online). Available: http://portal.sukabumikota.go.id/geografis/.

  • Badan Pusat Statistik. Statistik Lingkungan Hidup Indonesia (SLHI). 2018. Badan Pus. Stat. Indones. (2018) doi:3305001.

  • Central Bureau of Statistics. Indonesian Environmental Statistics . 2019. Badan Pus. Stat.


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  • Differentiation Roselle (Hibiscus Sabdariffa L.) Extract from Various Plants with FTIR-chemometric Method

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Authors

Mareetha Zahra S.
Department of Pharmaceutical Biology, Faculty of Pharmacy, Padjadjaran University, Jalan Raya Bandung- Sumedang KM 21, Jatinangor, West Java,, Indonesia
Yasmiwar Susilawati
Department of Pharmaceutical Biology, Faculty of Pharmacy, Padjadjaran University, Jalan Raya Bandung- Sumedang KM 21, Jatinangor, West Java,, Indonesia
Ida Musfiroh
Department of Pharmaceutical Analysis and Medicinal Chemistry, Faculty of Pharmacy, Padjadjaran University, Jalan Raya Bandung- Sumedang KM 21, Jatinangor, West Java,, Indonesia

Abstract


Background: Roselle prospectively can be developed as herbal medicine raw materials. The high amount availability of roselle raw material sources leads to diverse roselle extract quality therefore a particular method is required to differentiate roselle extracts. FTIR-chemometric is a method that is used to evaluate plant quality by processing chemical data information through mathematically and statistically calculations. Aim: The purpose of this study is to obtain data differentiation from all of the roselle extract obtained from various regions, identify from which region roselle extract has similar group with roselle standard extract, and identify the relation between roselle extracts quality with soil examination parameter. Materials and Method: Roselle simplisia collections were obtained from 12 regions which were Parangtritis, Nganjuk, Kediri, Ponorogo, Blitar, Bogor, Tulungagung, Boyolali, Yogyakarta, Sukabumi, Cileunyi, dan Malang. The extraction method used was using maceration with 70% ethanol. FTIR-chemometric was utilized to analyze. Results: Based on the results showed that FTIR-chemometric method can be used to differentiate roselle extract from several locations, roselle extract obtained from Tulungagung, Boyolali, and Sukabumi were in similar group with roselle extract standard, and roselle extract obtained from Tulungagung, Boyolali, and Sukabumi had similar soil examination parameter which were Phosphorus and Magnesium.

Keywords


Roselle, FTIR-chemometric, Soil parameter.

References