Open Access Open Access  Restricted Access Subscription Access

Mechanical Properties and Brittleness of Shale with Different Degrees of Fracturing-Fluid Saturation


Affiliations
1 College of Geosciences and Engineering, North China University of Water Resources and Electric Power, Zhengzhou 450045, China
2 Department of Civil and Environment Engineering, Colorado School of Mines, Golden 80401, United States
3 State Key Laboratory for Coal Mine Disaster Dynamics and Control, Chongqing University, Chongqing 400044, China
 

The mechanical characteristics of Longmaxi Formation shale with different degrees of fracturing-fluid saturation were characterized by applying triaxial compression tests at a confining pressure of 50 MPa. The test samples were collected from fresh outcrop shale in Dayou, Chongqing, China and the shale brittleness was evaluated based on brittleness-drop coefficient, stress decrease coefficient and softening modulus. The weakening of related rock parameters of shale specimens being immersed in fracturing-fluid for different time periods was studied and discussed. The degree of deterioration of the peak strengths, elastic and softening moduli and brittleness were significant and varied exponentially when the samples were soaked in fracturing-fluid. The samples were found to fail by shear on the whole accompanied by varying degrees of bedding plane cracking. With increase of sample immersion time, the number of shear failure surfaces changes from one to two and finally to more than three. The length and number of cracks parallel to bedding planes increased gradually, however, no cracks were formed perpendicular to the bedding plane even when the shale was soaked for a long time. The weakening of the brittleness and mechanical parameters with sample fracturing-fluid saturation are mainly related to change of stress state at the crack tips caused by hydration swelling, the dissolution caused by alkaline fracturing-fluid and the formation of liquid film on the surface of shale particles, all of which are the results of mechanical–physical–chemical coupling.

Keywords

Brittleness Evaluation Index, Hydration Swelling, Immersion Time, Longmaxi Formation Shale, Triaxial Compression, Weakening Mechanism.
User
Notifications
Font Size

  • Administration, USEI, Technically recoverable shale oil and shale gas resources: an assessment of 137 shale formations in 41 countries outside the United States, 2013.
  • Hou, Z. K., Yang, C. H., Guo, Y. T., Zhang, B. P., Wei, Y. L., Shuai, H. and Lei, W., Experimental study on anisotropic properties of longmaxi formation shale under uniaxial compression. Rock Soil Mech., 2015, 36, 2541–2550.
  • Jarvie, D., Evaluation of hydrocarbon generation and storage in Barnett shale, Fort worth basin, Humble Geochmeical Services Division, Texas, 2004.
  • Guo, Y., Yang, C., Jia, C., Jingbin, X. U., Lei, W. and Dan, L. I., Research on hydraulic fracturing physical simulation of shale and fracture characterization methods. Chin. J. Rock Mech. Eng., 2014, 33, 52–59.
  • Hou, Z. K., Yang, C. H., Lei, W., Liu, P. J., Guo, Y. T., Wei, Y. L. and Zhi, L. I., Hydraulic fracture propagation of shale horizontal well by large-scale true triaxial physical simulation test. Rock Soil Mech., 2016, 37, 0407–0414.
  • Liang, L., Xiong, J. and Liu, X., Experimental study on crack propagation in shale formations considering hydration and wettability. J. Nat. Gas Sci. Eng., 2015, 23, 492–499.
  • Tianshou, M. A. and Chen, P., Study of meso-damage characteristics of shale hydration based on ct scanning technology. Petrol. Exp. Dev., 2014, 41, 249–256.
  • Wen, H., Chen, M., Jin, Y., Wang, K., Xia, Y., Dong, J. and Niu, C., A chemo-mechanical coupling model of deviated borehole stability in hard brittle shale. Petrol. Exp. Dev., 2014, 41, 817–823.
  • Ma, T., Yang, C., Chen, P., Wang, X. and Guo, Y., On the damage constitutive model for hydrated shale using ct scanning technology. J. Nat. Gas Sci. Eng., 2016, 28, 204–214.
  • Han, Q., Chen, P. and Ma, T., Influencing factor analysis of shale microindentation measurement. J. Nat. Gas Sci. Eng., 2015, 27, 641–650.
  • Yan, Z., Xiang, X., Yan, J. and Wu, B., A novel drilling fluid with less free water. Petrol. Exp. Dev., 2011, 38, 490–494.
  • Zhong, H., Qiu, Z., Zhang, D., Tang, Z., Huang, W. and Wang, W., Inhibiting shale hydration and dispersion with amine-terminated polyamidoamine dendrimers. J. Nat. Gas Sci. Eng., 2016, 28, 52–60.
  • Younessi, A. and Rasouli, V., A fracture sliding potential index for wellbore stability analysis. Int. J. Rock Mech. Mining Sci., 2010, 47, 927–939.
  • Lomba, R. F. T., Chenevert, M. E. and Sharma, M. M., The role of osmotic effects in fluid flow through shales. J. Petrol. Sci. Eng., 2000, 25, 25–35.
  • Oort, E. V., On the physical and chemical stability of shales. J. Petrol. Sci. Eng., 2003, 38, 213–235.
  • Kang, Z. Q., Zhao, Y. S., Meng, Q. R., Yang, D. and Xi, B. P., Micro-ct experimental research of oil shale thermal cracking laws. Chin. J. Geophys., 2009, 52, 842–848.
  • Guancheng, J., Yourong, Q., Yuxiu, A., Xianbin, H. and Yanjun, R., Polyethyleneimine as shale inhibitor in drilling fluid. Appl. Clay Sci., 2016, 127–128, 70–77.
  • Shadizadeh, S. R., Moslemizadeh, A. and Dezaki, A. S., A novel nonionic surfactant for inhibiting shale hydration. Appl. Clay Sci., 2015, 118, 74–86.
  • Wang, P. and Qu, Z., NMR technology based hydration damage evolution of hard brittle shale. Rock Soil Mech., 2015, 36, 687–693.
  • Josh, M., Esteban, L., Piane, C. D., Sarout, J., Dewhurst, D. N.
  • and Clennell, M. B., Laboratory characterization of shale properties. J. Petrol. Sci. Eng., 2012, 88–89(2), 107–124.
  • Wu, X. Y., Baud, P. and Wong, T. F., Micromechanics of compressive failure and spatial evolution of anisotropic damage in darley dale sandstone. Int. J. Rock Mech. Min. Sci., 2000, 37, 143–160.
  • Wang, F. and Pan, Z., Numerical simulation of chemical potential dominated fracturing fluid flowback in hydraulically fractured shale gas reservoirs. Petrol. Exp. Dev., 2016, 43, 1060–1066.
  • Zou, C. et al., Shale gas in china: Characteristics, challenges and prospects (ii). Petrol. Exp. Dev., 2015, 43, 182–196.
  • Lu, Y. H., Chen, M., Jin, Y. and Zhang, G. Q., A mechanical model of borehole stability for weak plane formation under porous flow. Liq. Fuels Technol., 2012, 30, 1629–1638.
  • Wang, Y., Xiao, L. I., Yanfang, W. U., Yuxing, B., Shouding, L. I., Jianming, H. E. and Zhang, B., Research on relationship between crack initiation stress level and brittleness indices for brittle rocks. Chin. J. Rock Mech. Eng., 2014, 33(2), 264–275.
  • Hou, Z. K., Yang, C. H., Wei, X., Wang, L., Wei, Y. L., Xu, F. and Wang, H., Experimental study on the brittle characteristics of longmaxi formation shale. J. China Coal Soc., 2016, 41, 1188–1196.
  • Hucka, V. and Das, B., Brittleness determination of rocks by different methods. Int. J. Rock Mech. Min. Sci. Geomech. Abstracts, 1974, 11, 389–392.
  • Hou, Z. K., Yang, C. H., Wang, L. and Feng, X. U., Evaluation method of shale brittleness based on indoor experiments. J. Northeastern Univ., 2016, 37, 1496–1501.
  • Kahraman, S. and Altindag, R., A brittleness index to estimate fracture toughness. Int. J. Rock Mech. Min. Sci., 2004, 41, 343–348.
  • Qinghui, L. I., Chen, M., Yan, J., Wang, F. P., Bing, H. and Zhang, B., Indoor evaluation method for shale brittleness and improvement. Chin. J. Rock Mech. Eng., 2012, 31, 1680–1685.
  • Xu, F. et al., Effect of bedding planes on wave velocity and ae characteristics of the longmaxi shale in china. Arab. J. Geosci., 2017, 10, 141.
  • Hui, Z., Meng, F., Zhang, C., Rongchao, X. U. and Jingjing, L. U., Quantitative evaluation of rock brittleness based on stress-strain curve. Chin. J. Rock Mech. Eng., 2014, 33, 1114–1122.
  • Kang, Y., She, J., Lin, C. and You, L., Brittleness weakening mechanisms of shale soaked by drilling and completion fluid. Chin. J. Theoret. Appl. Mech., 2016, 48, 730–738.
  • GT/T23561-2009, The Professional Standards Compilation Group of Peoples Republic of China, Methods for determining the physical and mechanical properties of coal and rock. Standards Press of China, Beijing, 2009.
  • Wang, H., Guo, Y. T., Wang, L., Hou, Z. K. and Xu, F., An experimental study on mechanical anisotropy of shale reservoirs at different depths. Rock Soil Mech., 2017, 38, 2496–2506.
  • Arora, S. and Mishra, B., Investigation of the failure mode of shale rocks in biaxial and triaxial compression tests. Int. J. Rock Mech. Min. Sci., 2015, 79, 109–123.
  • Shi, G., Research on post-failure mechanical properties of brittleplastic rocks by OOFEM coupled with IEM. Doc. Diss., University of Chinese Academy of Sciences, 2005.
  • Zuo, J. et al., Study of energy-drop coefficient of brittle rock failure. Rock Soil Mech., 2014, 35(2), 321–327.
  • Obert, L. and Duvall, W. I., Rock Mechanics and the Design of Structures in Rock, John Wiley, Chichester, 1996, p. 649.
  • Shuai, H., Yang, C., Zhi, L. I., Lei, W. and Hou, Z., Shale brittleness estimation based on energy dissipation. J. Central South Univ., 2016.
  • Liu, X., Zeng, W., Liang, L. and Xiong, J., Experimental study on hydration damage mechanism of shale from the longmaxi formation in southern Sichuan basin, China. Petroleum, 2016, 2, 54–60.
  • Yang, S. L. and Wei, J. Z., Reservoir Physics, Petroleum Industry Press, Beijing, 2004.
  • Shuai, H., Yang, C., Guo, Y., Wang, C. and Lei, W., Influence of bedding planes on hydraulic fracture propagation in shale formations. Chin. J. Rock Mech. Eng., 2015, 34, 228–237.
  • Kang, Y., Chen, Q., You, L., Lin, C. and Cheng, Q., Laboratory studies of shale fracturing behaviors with rock-drilling fluid interactions, 2016, 40, 81–89.
  • You, L., Kang, Y., Chen, Z., Chen, Q. and Yang, B., Wellbore instability in shale gas wells drilled by oil-based fluids. Int. J. Rock Mech. Min. Sci., 2014, 72, 294–299.

Abstract Views: 396

PDF Views: 126




  • Mechanical Properties and Brittleness of Shale with Different Degrees of Fracturing-Fluid Saturation

Abstract Views: 396  |  PDF Views: 126

Authors

Zhenkun Hou
College of Geosciences and Engineering, North China University of Water Resources and Electric Power, Zhengzhou 450045, China
Marte Gutierrez
Department of Civil and Environment Engineering, Colorado School of Mines, Golden 80401, United States
Anming Wang
College of Geosciences and Engineering, North China University of Water Resources and Electric Power, Zhengzhou 450045, China
Abdulhadi Almrabat
Department of Civil and Environment Engineering, Colorado School of Mines, Golden 80401, United States
Chunhe Yang
State Key Laboratory for Coal Mine Disaster Dynamics and Control, Chongqing University, Chongqing 400044, China

Abstract


The mechanical characteristics of Longmaxi Formation shale with different degrees of fracturing-fluid saturation were characterized by applying triaxial compression tests at a confining pressure of 50 MPa. The test samples were collected from fresh outcrop shale in Dayou, Chongqing, China and the shale brittleness was evaluated based on brittleness-drop coefficient, stress decrease coefficient and softening modulus. The weakening of related rock parameters of shale specimens being immersed in fracturing-fluid for different time periods was studied and discussed. The degree of deterioration of the peak strengths, elastic and softening moduli and brittleness were significant and varied exponentially when the samples were soaked in fracturing-fluid. The samples were found to fail by shear on the whole accompanied by varying degrees of bedding plane cracking. With increase of sample immersion time, the number of shear failure surfaces changes from one to two and finally to more than three. The length and number of cracks parallel to bedding planes increased gradually, however, no cracks were formed perpendicular to the bedding plane even when the shale was soaked for a long time. The weakening of the brittleness and mechanical parameters with sample fracturing-fluid saturation are mainly related to change of stress state at the crack tips caused by hydration swelling, the dissolution caused by alkaline fracturing-fluid and the formation of liquid film on the surface of shale particles, all of which are the results of mechanical–physical–chemical coupling.

Keywords


Brittleness Evaluation Index, Hydration Swelling, Immersion Time, Longmaxi Formation Shale, Triaxial Compression, Weakening Mechanism.

References





DOI: https://doi.org/10.18520/cs%2Fv115%2Fi6%2F1163-1173