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Growth and Characterization of P-Chloroanilinepthalic Acid Single Crystals


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1 Department of Science & Humanities, M. Kumarasamy College of Engineering, Karur, Tamil Nadu, India
     

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P-CaP (p-chloroanilinepthalic acid) single crystal was grown by slow evaporation technique. A single Crystal XRD study reveals that the grown crystal belongs to orthorhombic system. Decomposition mechanism and melting point of the sample were deliberated in TGA/DSC analysis. Transmission ability of the crystal in the visible was tested by recording UV-VIS-NIR spectrum also Mechanical strength of the material is determined by Vickers hardness test. The FTIR Spectrum was recorded in the range of 400 cm-1 and 4000 cm-1 which is confirmed the formation of p-CaP crystal.

Keywords

Optical Analysis, Single Crystal, XRD.
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  • Growth and Characterization of P-Chloroanilinepthalic Acid Single Crystals

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Authors

J. Vidhya
Department of Science & Humanities, M. Kumarasamy College of Engineering, Karur, Tamil Nadu, India
R. Padmavathi
Department of Science & Humanities, M. Kumarasamy College of Engineering, Karur, Tamil Nadu, India

Abstract


P-CaP (p-chloroanilinepthalic acid) single crystal was grown by slow evaporation technique. A single Crystal XRD study reveals that the grown crystal belongs to orthorhombic system. Decomposition mechanism and melting point of the sample were deliberated in TGA/DSC analysis. Transmission ability of the crystal in the visible was tested by recording UV-VIS-NIR spectrum also Mechanical strength of the material is determined by Vickers hardness test. The FTIR Spectrum was recorded in the range of 400 cm-1 and 4000 cm-1 which is confirmed the formation of p-CaP crystal.

Keywords


Optical Analysis, Single Crystal, XRD.

References