Manufacturing Technology Today

Open Access Open Access  Restricted Access Subscription Access
Open Access Open Access Open Access  Restricted Access Restricted Access Subscription Access

Heat treatment of plasma sprayed tricalcium phosphate coatings deposited on substrate Ti-6Al-4V ELI


Affiliations
1 Indian Institute of Technology Indore, Indore, India, India
2 ndian Institute of Technology Patna, Patna, India, India
     

   Subscribe/Renew Journal


Micron-sized spray-dried tricalcium phosphate (TCP) powder has been deposited successfully on the substrate of Ti-6Al-4V ELI alloy through an atmospheric plasma spraying process. Further, heat treatment of the deposited coating is carried out at a temperature of 600 ℃ for the holding time duration of 2 h in a muffle furnace. Phase identification of the as-deposited and post heat-treated TCP coatings is analyzed through an X-ray diffractometer (XRD). The top morphology and microstructure of both coatings are examined with the help of the field emission scanning electron microscope (FESEM). The porosity and micro-crack are found to be reduced by heat treatment. Fully molten particles are noticed to be dominant on the top surface of the coating obtained after performing heat treatment. The transformation of secondary phases, namely tetra calcium phosphate (TTCP) and calcium oxide, into stable tricalcium phosphate is achieved by heat treatment.

Keywords

Tricalcium Phosphate, Atmospheric Plasma Spraying Process, Heat Treatment, XRD, FESEM.
User
Subscription Login to verify subscription
Notifications
Font Size

  • Bai, X., More, K., Rouleau, C. M., & Rabiei, A. (2010). Functionally graded hydroxyapatite coatings doped with antibacterial components. Acta Biomaterialia, 6(6), 2264-2273. https://doi.org/10.1016/j.actbio.2009.12.002

  • Chen, X., Ji, G., Bai, X., Yao, H., Chen, Q., & Zou, Y. (2018). Microstructures and Properties of Cold Spray Nanostructured HA Coatings. Journal of Thermal Spray Technology, 27(8), 1344-1355. https://doi.org/10.1007/s11666-018-0776-1

  • Farnoush, H., Aldıç, G., & Çimenoğlu, H. (2015). Functionally graded HA–TiO2 nanostructured composite coating on Ti–6Al–4V substrate via electrophoretic deposition. Surface and Coatings Technology, 265, 7-15. https://doi. org/10.1016/j.surfcoat.2015.01.069

  • Gligorijević, B. R., Vilotijević, M., Šćepanović, M., Vidović, D., & Radović, N. A. (2016). Surface structural heterogeneity of high power plasmasprayed hydroxyapatite coatings. Journal of Alloys and Compounds, 687, 421-430. https:// doi.org/10.1016/j.jallcom.2016.06.163

  • Hussain, S., & Sabiruddin, K. (2021a). Synthesis of eggshell based hydroxyapatite using hydrothermal method. IOP Conference Series: Materials Science and Engineering, 1189(1), 012024.https://doi.org/10.1088/1757-899x/ 1189/1/012024

  • Hussain, S., & Sabiruddin, K. (2021b). Effect of heat treatment on the synthesis of hydroxyapatite from Indian clam seashell by hydrothermal method. Ceramics International, 47(21), 29660-29669. https://doi.org/10.1016/j. ceramint.2021.07.137

  • Hussain, S., Shah, Z. A., Sabiruddin, K., & Keshri, A. K. (2023). Characterization and tribological behaviour of Indian clam seashell-derived hydroxyapatite coating applied on titanium alloy by plasma spray technique. Journal of the Mechanical Behavior of Biomedical Materials, 137, 105550. https://doi.org/10.1016/j.jmbbm.

  • 105550

  • Hussain, S., Sharma, M., Sharma, V., Brahmane, S., & Sabiruddin, K. (2022). Effect of Ni-5Al Addition on the Properties of BaAl2O4-Based Coating Deposited with a Novel Explosive Spray Coating Technique. Journal of Thermal Spray Technology. https://doi.org/10.1007/s11666022-01492-z

  • Jafari, H., Hessam, H., Shahri, S. M. G., Assadian, M., Shairazifard, S. H. P., & Idris, M. H. (2016).

  • Characterizing Sintered Nano-Hydroxyapatite Sol-Gel Coating Deposited on a Biomedical Ti-Zr-Nb Alloy. Journal of Materials Engineering and Performance, 25(3), 901-909. https://doi. org/10.1007/s11665-016-1944-4

  • Li, H., Khor, K. A., & Cheang, P. (2002). Properties of heat-treated calcium phosphate coatings deposited by high-velocity oxy-fuel (HVOF) spray. Biomaterials, 23(10), 2105-2112. https:// doi.org/10.1016/S0142-9612(01)00326-X

  • Mejias, A., Candidato, R. T., Pawłowski, L., & Chicot, D. (2016). Mechanical properties by instrumented indentation of solution precursor plasma sprayed hydroxyapatite coatings: Analysis of microstructural effect. Surface and Coatings Technology, 298, 93-102. https://doi.org/10.1016/j.surfcoat.2016.04.028

  • Morks, M. F. (2008). Fabrication and characterization of plasma-sprayed HA / SiO2 coatings for biomedical application. Journal of the Mechanical Behavior of Biomedical Materials, 1(1), 105-111.https://doi.org/10.1016/j.jmbbm.2007.04.003

  • Nelea, V., Ristoscu, C., Chiritescu, C., Ghica, C., Mihailescu, I. N., Pelletier, H., Mille, P., & Cornet, A.

  • (2000). Pulsed laser deposition of hydroxyapatite thin films on Ti-5Al-2.5Fe substrates with and without buffer layers. Applied Surface Science, 168(1-4), 127-131. https://doi.org/10.1016/ S0169-4332(00)00616-4

  • Pei, L., Zhang, B., Luo, H., Wu, X., Li, G., Sheng, H., & Zhang, L. (2019). Electrodeposition of ZnO Nanoprism-Zn substituted hydroxyapatite duplex layer coating for carbon fiber. Ceramics International, 45(11), 14278-14286. https://doi. org/10.1016/j.ceramint.2019.04.137

  • Surmeneva, M. A., Tyurin, A. I., Mukhametkaliyev, T. M., Pirozhkova, T. S., Shuvarin, I. A., Syrtanov, M. S., & Surmenev, R. A. (2015). Enhancement of the mechanical properties of AZ31 magnesium alloy via nanostructured hydroxyapatite thin films fabricated via radio-frequency magnetron sputtering. Journal of the Mechanical Behavior of Biomedical Materials, 46, 127-136. https:// doi.org/10.1016/j.jmbbm.2015.02.025

  • Vahabzadeh, S., Roy, M., Bandyopadhyay, A., & Bose, S. (2015). Phase stability and biological property evaluation of plasma sprayed hydroxyapatite coatings for orthopedic and dental applications.

  • Acta Biomaterialia, 17, 47-55. https://doi. org/10.1016/j.actbio.2015.01.022

  • Xu, H., Geng, X., Liu, G., Xiao, J., Li, D., Zhang, Y., Zhu, P., & Zhang, C. (2016). Deposition, nanostructure

  • and phase composition of suspension plasmasprayed hydroxyapatite coatings. Ceramics

  • International, 42(7), 8684-8690. https://doi.org/10.1016/j.ceramint.2016.02.102

  • Yao, H. L., Ji, G. C., Chen, Q. Y., Bai, X. B., Zou, Y. L., & Wang, H. T. (2018). Microstructures and

  • Properties of Warm-Sprayed Carbonated Hydroxyapatite Coatings. Journal of ThermalSpray Technology, 27(6), 924-937. https://doi. org/10.1007/s11666-018-0735-x

  • Yuan, Q., Qin, C., Wu, J., Xu, A., Zhang, Z., Liao, J., Lin, S., Ren, X., & Zhang, P. (2016). Synthesis

  • and characterization of Cerium-doped hydroxyapatite/polylactic acid composite coatings on metal substrates. Materials Chemistry and Physics, 182, 365-371. https://

  • doi.org/10.1016/j.matchemphys.2016.07.044


Abstract Views: 126

PDF Views: 1




  • Heat treatment of plasma sprayed tricalcium phosphate coatings deposited on substrate Ti-6Al-4V ELI

Abstract Views: 126  |  PDF Views: 1

Authors

Shahid Hussain
Indian Institute of Technology Indore, Indore, India, India
Anup Kumar Keshri
ndian Institute of Technology Patna, Patna, India, India
Kazi Sabiruddin
Indian Institute of Technology Indore, Indore, India, India

Abstract


Micron-sized spray-dried tricalcium phosphate (TCP) powder has been deposited successfully on the substrate of Ti-6Al-4V ELI alloy through an atmospheric plasma spraying process. Further, heat treatment of the deposited coating is carried out at a temperature of 600 ℃ for the holding time duration of 2 h in a muffle furnace. Phase identification of the as-deposited and post heat-treated TCP coatings is analyzed through an X-ray diffractometer (XRD). The top morphology and microstructure of both coatings are examined with the help of the field emission scanning electron microscope (FESEM). The porosity and micro-crack are found to be reduced by heat treatment. Fully molten particles are noticed to be dominant on the top surface of the coating obtained after performing heat treatment. The transformation of secondary phases, namely tetra calcium phosphate (TTCP) and calcium oxide, into stable tricalcium phosphate is achieved by heat treatment.

Keywords


Tricalcium Phosphate, Atmospheric Plasma Spraying Process, Heat Treatment, XRD, FESEM.

References