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Synthesis and Spectral Investigation of Heterocycles Containing Di and Tri-Heteroatoms


Affiliations
1 Dept. of Chem., Educt. College, Kufa Univ., Iraq
2 Dept of Chem., Science College, Babylon Univ., Iraq
3 College of Pharmacy, Univ. Kufa, Iraq
     

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The aim of this work, synthesis of mono cycles containing di and tri-hetero atoms from((N, S, O and Se) via reaction between di ester compounds with di hetero atoms compounds like (alkyl di amine, ethylene glycol, ethylene di thiol, sodium hydro selenium with di chloro ethylene)., and synthesis some of them via reaction of di carbonyl compounds with di hetero atoms compounds to give cycles included two or more heteroatoms (N, S, O and Se) by several steps via condensation reactions. All formatted compounds have been investigated using several spectral techniques (elemental analysis (C.H.N), H.NMR-spectra, FT.IR-spectra) and measurement of melting points.

Keywords

Alkyl Di Amine, Tri Heteroatoms, Sodium Hydride, Alkyl Dichloride.
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  • Synthesis and Spectral Investigation of Heterocycles Containing Di and Tri-Heteroatoms

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Authors

Nagham Mahmood Aljamali
Dept. of Chem., Educt. College, Kufa Univ., Iraq
Shireen Ridha Rasool
Dept of Chem., Science College, Babylon Univ., Iraq
Rana Neama Atiya
College of Pharmacy, Univ. Kufa, Iraq

Abstract


The aim of this work, synthesis of mono cycles containing di and tri-hetero atoms from((N, S, O and Se) via reaction between di ester compounds with di hetero atoms compounds like (alkyl di amine, ethylene glycol, ethylene di thiol, sodium hydro selenium with di chloro ethylene)., and synthesis some of them via reaction of di carbonyl compounds with di hetero atoms compounds to give cycles included two or more heteroatoms (N, S, O and Se) by several steps via condensation reactions. All formatted compounds have been investigated using several spectral techniques (elemental analysis (C.H.N), H.NMR-spectra, FT.IR-spectra) and measurement of melting points.

Keywords


Alkyl Di Amine, Tri Heteroatoms, Sodium Hydride, Alkyl Dichloride.