Indian Journal of Pure and Applied Physics

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Synthesis of Iron Oxide Nanoparticles from Scrapped Waste Materials for Efficient Dye Removal to Purify Industrial Waste Water


Affiliations
1 Department of Chemistry, School of Physical Sciences, Jawaharlal Nehru University, New Delhi 110 067, India
 

In this investigation, we used a circular economy approach by recycling metal scrap from industry as a component in creating nanoparticles. For producing iron oxide NPs we used electrochemical method with scrapped rusted iron nails as electrodes. In this technique, we used 50mM ferrous sulphate solution as an electrolyte and a direct current power supply. Different methods were used to characterise the synthesised iron oxide NPs, including ultraviolet-visible (UV-visible) spectroscopy, Fourier transform infrared (FTIR) spectroscopy, X-ray diffraction (XRD), and transmission electron microscopy (TEM). The results demonstrated that the synthesised iron oxide NPs have an average crystallite size of 7.54 nm. Iron oxide NPs has potential to adsorb Congo red dye hence prepared NPs have been utilised for the adsorption of Congo red dye.

Keywords

Nanoparticles; Waste materials; TEM; UV-Vis; Dye removal.
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  • Sahoo A & Patra S , ACS Appl Nano Mater, 1 (2018) 5169.

  • Sharma J & Janveja B, RJC Rasayan J Chem, 1 (2008) 936.

  • Kishor R, et al, Environ Technol Innov, 22 (2021) 101425

  • Cao J, Sanganyado E, Liu W, Zhang W & Liu Y, J Environ Manage, 242 (2019) 229.

  • Arruda E H, Andrade R, Melatto P B, Levy W & De Melo Conti D, Sustain Oper Comput, 2 (2021) 79.

  • Saini J, Garg V K, Gupta R K & Kataria N, J Environ Chem Eng, 5 (2017) 884.

  • Anastopoulos I, Hosseini-Bandegharaei A, Fu J, Mitropoulos A C & Kyzas G Z, Rev J Dispers Sci Technol, 39 (2018) 836.

  • Joshi S, Garg V K, Kataria N & Kadirvelu K,Chemosphere, 236 (2019) 124280.

  • Wang F, et al, Mater Sci Semicond Process, 16 (2013) 802.

  • Bokuniaeva A O & Vorokh A S, J Phys Conf Ser, 1410 (2019) 012057.


Abstract Views: 57

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  • Synthesis of Iron Oxide Nanoparticles from Scrapped Waste Materials for Efficient Dye Removal to Purify Industrial Waste Water

Abstract Views: 57  |  PDF Views: 31

Authors

Virender Kumar
Department of Chemistry, School of Physical Sciences, Jawaharlal Nehru University, New Delhi 110 067, India
Akash Barala
Department of Chemistry, School of Physical Sciences, Jawaharlal Nehru University, New Delhi 110 067, India
Vijay Kumar Goel
Department of Chemistry, School of Physical Sciences, Jawaharlal Nehru University, New Delhi 110 067, India

Abstract


In this investigation, we used a circular economy approach by recycling metal scrap from industry as a component in creating nanoparticles. For producing iron oxide NPs we used electrochemical method with scrapped rusted iron nails as electrodes. In this technique, we used 50mM ferrous sulphate solution as an electrolyte and a direct current power supply. Different methods were used to characterise the synthesised iron oxide NPs, including ultraviolet-visible (UV-visible) spectroscopy, Fourier transform infrared (FTIR) spectroscopy, X-ray diffraction (XRD), and transmission electron microscopy (TEM). The results demonstrated that the synthesised iron oxide NPs have an average crystallite size of 7.54 nm. Iron oxide NPs has potential to adsorb Congo red dye hence prepared NPs have been utilised for the adsorption of Congo red dye.

Keywords


Nanoparticles; Waste materials; TEM; UV-Vis; Dye removal.

References